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Low temperature carburizing of a series of austenitic stainless with various combinations of chromium and nickel equivalents was performed. The investigation of the response towards low temperature carburized for three stainless steels with various Cr- and Ni-equivalents showed that the carbon uptake depends significantly on the chemical composition of the base material. The higher carbon content in the expanded austenite layer of specimen 6 (1.4565) and specimen 4 (1.4539/AISI 904L) compared to specimen 2 (1.4404/AISI 316L) is assumed to be mainly related to the difference in the specimens’ chromium content. More chromium leads to more lattice expansion. Along with the higher carbon content, higher hardness values and higher compressive residual stresses in the expanded austenite zone are introduced than for low temperature carburized AISI 316L. The residual stresses obtained from X-ray diffraction lattice strain investigation depend strongly on the chosen X-ray elastic constants. Presently, no values are known for carbon (or nitrogen) stabilized expanded austenite. Nevertheless, first principle elastic constants for γ′&minus Fe4C appear to provide realistic residual stress values. Magnetic force microscopy and measurement with an eddy current probe indicate that austenitic stainless steels can become ferromagnetic upon carburizing, similar for low temperature nitriding. The apparent transition from para- to ferromagnetism cannot be attributed entirely to the interstitially dissolved carbon content in the formed expanded austenite layer but appears to depend also on the metallic composition of the alloy, in particular the Ni content.
Thermochemical surface hardening is used to overcome the weak mechanical performance of austenitic and duplex stainless steels. Both low-temperature carburizing and nitrocarburizing can improve the hardness, wear, galling, and cavitation resistance, while maintaining their good corrosion resistance. Therefore, it is crucial to not form chromium-rich precipitates during hardening as these can deteriorate the passivity of the alloy. The hardening parameters, the chemical composition of the steel, and the manufacturing route of a component determine whether precipitates are formed. This article gives an overview of suitable alloys for low-temperature surface hardening and the performance under corrosive loading.
Thermal shape memory alloys show extraordinary material properties and can be used as actuators, dampers and sensors. Since their discovery in the middle of the last century they have been investigated and further developed. The majority of the industrial applications with the highest material sales can still be found in the medical industry, where they are used due to their superelastic and thermal shape memory effect, e.g. as stents or as guidewires and tools in the minimal invasive surgery. Particularly in recent years, more and more applications have been developed for other industrial fields, e.g. for the household goods, civil engineering and automotive sector. In this context it is worth mentioning that for the latter sector, million seller series applications have found their way into some European automobile manufacturers. The German VDI guideline for shape memory alloys introduced in 2017 will give the material a further boost in application. Last but not least the new production technologies of additive manufacturing with metal laser sintering plants open up additional applications for these multifunctional materials. This paper gives an overview of the extraordinary material properties of shape memory components, shows examples of different applications and discusses European trends against the background of the most recent standard and new production technologies.
The project aims for the development of a new material system from high tensile stainless steel wires as net material with environmentally compatible antifouling properties for off-shore fish farm cages. Therefore, current net materials from textiles (polyamide) shall be partially replaced by high strength stainless steel in order to have a more environmentally compatible system which meets the more severe mechanical loads (waves, storms, predators (sharks)). With a new antifouling strategy current issues like reduced ecological damage (e.g. due to copper disposal), lower maintenance costs (e.g. cleaning) and reduced durability shall be resolved.
Martensitic stainless steels has a wide use, for example for blades, knifes or cutter. The best corrosion resistance of these materials is in hardened condition. For better mechanical properties a tempering is normally applied to increase the durability. The tempering is also reducing the hardness and finally the corrosion resistance. Austempering is meanly used at low alloyed steels and brings a good compromise between durability, hardness and corrosion resistance. For martensitic stainless steels, austempering is normally not a topic because of the very long tempering times.
This work shows first results of austempering of some standard martensitic stainless steels and the influence to corrosion resistance. For reference, hardened and also hardened and tempered specimens were investigated. The corrosions resistance was investigated by electrochemical methods.
Magnetic effects on austenitic stainless steels, formed during a low temperature carburizing depending on the alloy composition are discussed in this paper. Samples of different austenitic stainless steel alloys have been subjected to a multiple low-temperature carburization. Layer characteriszation with light microscope and hardness profiles show a growth of the layer thickness. The formation of an expanded austenite layer (lattice expansion) could be detected by X-ray diffraction (XRD). Feritscope was used to determine the magnetizability, whereby not all austenitic alloys form a magnetizability after treatment. Furthermore, test procedures were developed to visualize the magnetizability. For this purpose, magnetic force microscope measurements and investigations with ferrofluid were carried out and a fir tree ferromagnetic layer strucure could be proven.
The first part of this work shows the development and application of a new material system using high strength duplex stainless steel wires as net material with environmentally compatible antifouling properties for off-shore fish farm cages. Current net materials from textiles (polyamide) shall be partially replaced by high strength duplex stainless steel in order to have a more environmentally compatible system which meets the more severe mechanical loads (waves, storms, predatores (sharks, seals)). With a new antifouling strategy current issues like reduced ecological damage (e.g. due to copper disposal), lower maintenance costs (e.g. cleaning) and reduced durability shall be resolved.
High strength steel wires are also widely used in geological protection systems, for example rockfall protection or slope stabilisation. Normally hot-dip galvanised carbon steel is used in this case. But in highly corrosive environments like coastal areas, volcanic areas or mines for example, other solutions with a high corrosion resistance and sufficient mechanical properties are necessary. Protection systems made of high strength duplex stainless steel wires enable a significantly longer service life of the portection systems and therefore a higher level of security.
Pitting susceptibility of metastable austenitic stainless steels as a function of surface conditions
(2019)
The influence of surface roughness and local defects on pitting susceptibility of type 304 (UNS S30400) and type 301 (UNS S30100) in chloride solution were investigated. Because the mechanical properties can be regarded as decisive for the achieved surface quality, different properties of the base material were obtained by cold rolling the metastable austenites. This was done before the surfaces were finished. Therefor the surfaces were treated by different grinding parameters to generate different surface conditions and different defects. As a reference, different standardised surface finishes were used.
By using and comparing different methods for the characterization of surface roughness and surface texture, it is possible to find a relationship between the quantity and characteristics of local defects on the one hand and pitting susceptibility on the other hand. For the machining parameters used, a ranking of the influencing factors on the corrosion resistance achieved could be determined.
The automated application of software-based solutions for estimating the pitting susceptibility of machined surfaces and components will be discussed using concrete examples.