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Thermochemical surface hardening is used to overcome the weak mechanical performance of austenitic and duplex stainless steels. Both low-temperature carburizing and nitrocarburizing can improve the hardness, wear, galling, and cavitation resistance, while maintaining their good corrosion resistance. Therefore, it is crucial to not form chromium-rich precipitates during hardening as these can deteriorate the passivity of the alloy. The hardening parameters, the chemical composition of the steel, and the manufacturing route of a component determine whether precipitates are formed. This article gives an overview of suitable alloys for low-temperature surface hardening and the performance under corrosive loading.
The project aims for the development of a new material system from high tensile stainless steel wires as net material with environmentally compatible antifouling properties for off-shore fish farm cages. Therefore, current net materials from textiles (polyamide) shall be partially replaced by high strength stainless steel in order to have a more environmentally compatible system which meets the more severe mechanical loads (waves, storms, predators (sharks)). With a new antifouling strategy current issues like reduced ecological damage (e.g. due to copper disposal), lower maintenance costs (e.g. cleaning) and reduced durability shall be resolved.
Martensitic stainless steels has a wide use, for example for blades, knifes or cutter. The best corrosion resistance of these materials is in hardened condition. For better mechanical properties a tempering is normally applied to increase the durability. The tempering is also reducing the hardness and finally the corrosion resistance. Austempering is meanly used at low alloyed steels and brings a good compromise between durability, hardness and corrosion resistance. For martensitic stainless steels, austempering is normally not a topic because of the very long tempering times.
This work shows first results of austempering of some standard martensitic stainless steels and the influence to corrosion resistance. For reference, hardened and also hardened and tempered specimens were investigated. The corrosions resistance was investigated by electrochemical methods.
Magnetic effects on austenitic stainless steels, formed during a low temperature carburizing depending on the alloy composition are discussed in this paper. Samples of different austenitic stainless steel alloys have been subjected to a multiple low-temperature carburization. Layer characteriszation with light microscope and hardness profiles show a growth of the layer thickness. The formation of an expanded austenite layer (lattice expansion) could be detected by X-ray diffraction (XRD). Feritscope was used to determine the magnetizability, whereby not all austenitic alloys form a magnetizability after treatment. Furthermore, test procedures were developed to visualize the magnetizability. For this purpose, magnetic force microscope measurements and investigations with ferrofluid were carried out and a fir tree ferromagnetic layer strucure could be proven.
The first part of this work shows the development and application of a new material system using high strength duplex stainless steel wires as net material with environmentally compatible antifouling properties for off-shore fish farm cages. Current net materials from textiles (polyamide) shall be partially replaced by high strength duplex stainless steel in order to have a more environmentally compatible system which meets the more severe mechanical loads (waves, storms, predatores (sharks, seals)). With a new antifouling strategy current issues like reduced ecological damage (e.g. due to copper disposal), lower maintenance costs (e.g. cleaning) and reduced durability shall be resolved.
High strength steel wires are also widely used in geological protection systems, for example rockfall protection or slope stabilisation. Normally hot-dip galvanised carbon steel is used in this case. But in highly corrosive environments like coastal areas, volcanic areas or mines for example, other solutions with a high corrosion resistance and sufficient mechanical properties are necessary. Protection systems made of high strength duplex stainless steel wires enable a significantly longer service life of the portection systems and therefore a higher level of security.
Pitting susceptibility of metastable austenitic stainless steels as a function of surface conditions
(2019)
The influence of surface roughness and local defects on pitting susceptibility of type 304 (UNS S30400) and type 301 (UNS S30100) in chloride solution were investigated. Because the mechanical properties can be regarded as decisive for the achieved surface quality, different properties of the base material were obtained by cold rolling the metastable austenites. This was done before the surfaces were finished. Therefor the surfaces were treated by different grinding parameters to generate different surface conditions and different defects. As a reference, different standardised surface finishes were used.
By using and comparing different methods for the characterization of surface roughness and surface texture, it is possible to find a relationship between the quantity and characteristics of local defects on the one hand and pitting susceptibility on the other hand. For the machining parameters used, a ranking of the influencing factors on the corrosion resistance achieved could be determined.
The automated application of software-based solutions for estimating the pitting susceptibility of machined surfaces and components will be discussed using concrete examples.
Mechanical properties after stretching testings were calcu-lated and experimentally determined via Tempcore method for bar core, bar surface and whole bar cross section. It was displayed on the base of experiments and imitating simulation that deformation in core and surface areas of a bar are equal and therefore influence of structural parameters in the core area is principally decisive for initiating of neck forming in the surface area. The results showed that resistance to destruction of martensite surface layer has rather less effect on bar properties in general in comparison with previous investigations. It is concluded that improvement of core structure quality can help to lower brittleness of the whole bar. It was also proved that used techniques provide good concordance between the obtained results and experimental data. Therefore, the additivity rule for structural components can be used successfully for determination of whole bar parameters, taking into account thickness of surface layer that can be measured easily using hardness sensor. It will simplify practically quality control of products.
Investigation of magnetic effects on austenitic stainless steels after low temperature carburization
(2018)
This work aims at investigating the magnetic effects of austenitc stainless steels which can occur after a low temperature carburisation depending on the alloy. Samples were prepared of different alloys and subjected to a multiple low temperature carburisation to obtain different treatment conditions for each alloy. The layer characterisation was carried out by light microscope and also by hardening profiles and shows that the layer develops with each additional treatment cycle. A lattice expansion could be detected in all treated samples by X-ray diffraction. Magnetisability was measured using Feritscope and SQUID measurements. Not all alloys showed magnetisability after treatment. In addition to MFM measurements, experiments with Ferrofluid were also used to visualize the magnetic areas. These studies show that only about half of the formed layer becomes magnetisable and has a domain-like structure.
In Anlehnung an das Tempcore-Verfahren wurde an wärmebehandeltem Stabstahl das Zugverfestigungsverhalten des Kernes, der Außenhaut sowie dem gesamten Stab experimentell und numerisch ermittelt. Es zeigte sich, dass die Dehnungen am Kern und am äußeren Rand gleich sind und der Einfluss des Kerngefüges entscheidend für den Beginn der Einschnürung in der Außenhaut ist. Eine Verbesserung der Eigenschaften des Kerngefüges kann somit die Bruchempfindlichkeit des gesamten Stabes reduzieren.
Formgedächtnislegierungen
(2018)
Formgedächtnislegierungen sind »Legierungen, die nach geeigneter Behandlung aufgrund einer martensitischen Umwandlung ihre Gestalt in Abhängigkeit von der Temperatur ändern«. Derartige Materialien werden in den nächsten Jahrzehnten eine wachsende Rolle in der Technik spielen. Um die Eigenschaften dieser Werkstoffe optimal nutzen zu können, ist es wichtig, den Einfluss des Herstellungs- und Verarbeitungsprozesses auf ihre Anwendung zu kennen.
Das Buch behandelt die metallkundlichen Hintergründe und die Verwendungsmöglichkeiten der Formgedächtnislegierungen in verständlicher, auf den Anwender zugeschnittener Weise.
The electrochemical behavior for different surface conditions and different degrees of deformation of metastable austenitic stainless steel AISI 304 UNS S30400 were studied using critical pitting potential and electrochemical noise measurements. The influence on corrosion resistance by using different abrasives (silicon carbide and corundum) for surface finish by grinding is illustrated. For the characterization of local defects and surface topography, scanning electron microscopy (SEM) and tactile measurements were used. An inverse correlation between occurrence of local defects on the surface and critical pitting potential was found by using image processing. Therefore, gray scale values of different surfaces were compared. The influence of mass content of α'-martensite on the corrosion resistance is shown by comparing different qualities of surface finish. For smooth machined surfaces it can be shown that an increasing numbers of strain induced martensite is decreasing the corrosion resistance lightly. For low abrasive machining an inverse correlation between the critical pitting potential and surface roughness is given. However, for higher abrasive machining parameters, this correlation could not be found.
Durch Beanspruchungen bei der Fertigung oder in der Anwendung können metastabile austenitische Stähle eine Phasenumwandlung von ?- Austenit zu ?‘-Martensit durchlaufen. Verbunden damit sind Eigenschaftsänderungen, welche sich signifikant auf das Werkstoffverhalten unter mechanischer, tribologischer oder korrosiver Belastung auswirken können.
Um möglichen negativen Auswirkungen wie ungewollte Magnetisierbarkeit oder Beeinflussung von Fertigungsparameter sowie Korrosionseigenschaften zu unterbinden muss die martensitische Phase zunächst erfasst und quantifiziert werden.
Für diese Aufgabe stehen neben den bekannten und kostenintensiven Verfahren wie EBSD und XRD für die praxisnahe Anwendung das magneto-induktive Messverfahren und verschiedene Ätzmethoden zur Verfügung.
Anhand von Applikationen aus Anwendung, Fertigung und Forschung werden die Wirkweisen, Vorteile und Grenzen verschiedener Ätzverfahren und dem magneto-induktiv messenden FERITSCOPE® MP30 aufgezeigt. Ebenso werden ergänzende Methoden bzw. Techniken zur Validation der Verfahren diskutiert und erläutert.
In the automotive industry a strong effort has been undertaken to reduce the weight of modern vehicles. In order to reduce the energy consumption and to improve the environmental sustainability, the importance of weight reduction activities is even growing faster. As lightweight designing is becoming more and more expensive and show less potential savings, new approaches are needed. One promising technology could be the use of shape memory elements. In the last years a lot of potential application possibilities were presented, demonstrating the benefit of these functional elements in automotive design solutions: they often reduce complexity, weight and design space of an actuation device and enable new functions. In addition they work silently and are therefore ideally suitable for comfort applications in the passenger cabin. Because of the current trend to electric vehicle the hitherto existing drawback of a high electrical energy consumption of shape memory actuators in some design proposals is not given any more.